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Beilstein J. Org. Chem. 2020, 16, 1296–1304, doi:10.3762/bjoc.16.110
Graphical Abstract
Figure 1: Phthalimide derivatives 1–3 and the corresponding azomethine ylides 1AMY-3AMY.
Scheme 1: Irradiation of 1 in the presence of acrylonitrile (AN).
Figure 2: Dependence of the chemical shift of the H-atom at the cyclohexane 2 position in compound 2 on the β...
Scheme 2: Complexation of 2 with β-CD, and formation of a ternary complex AN@2@β-CD.
Scheme 3: Photochemistry of 2 in the presence of AN, with or without β-CD.
Scheme 4: Photochemistry of 3 in the presence of AN, with or without β-CD.
Beilstein J. Org. Chem. 2011, 7, 270–277, doi:10.3762/bjoc.7.36
Scheme 1: Photoinduced domino reaction of adamantylphthalimide.
Scheme 2: Synthesis of homoadamantylphthalimide 5.
Figure 1: Molecular structure of 5, the geometry optimization was performed by use of DFT B3LYP/6-31G.
Scheme 3: Products after irradiation of 5.
Scheme 4: Proposed mechanism for the photochemical transformation of 5.